Právní předpis byl sestaven k datu 31.07.2016.
Zobrazené znění právního předpisu je účinné od 30.11.2005 do 31.07.2016.
Vyhláška o metodách zkoušení a způsobu odběru a přípravy kontrolních vzorků
211/2004 Sb.
1. xxxxxxxxx, poškozených xxxx xxxxx závadných; xxxx xxxxx xxxxx se xxxxxx x vzorek xx xxxxxxxx se x xxxx neodebírá, xxxxx xx xxxxxxx x podezřelou xxxxxxxxx, xxx se xxxxxxxxx xxxxx odstavce 12,
2. xxxxxxxxxxx; x xxxxx xxxxxxxxxx části xxxxx xx odebírají xxxxxx xxxxxxxxxx.
1. xxxxxxxx xxxxx xxxxx §3 xxxx. 2 xxxx. x),
2. rozsah nebo xxxxxxxx xxxxxxxxxx xxxxx; x xxxxxxxx xxxxxxxxx xxxxx jednotek xxxxxx xxxx xxxxxx xxxxxxxx, x nekusové potraviny xxxxxxx xxxxxxxx xxxx xxxxx,
3. datum xxxxxx, xx-xx uvedeno,
4. datum xxxxxxxxxxxxx nebo xxxxx xxxxxxxxx xxxxxxxxxxxx;
1. xxxxx xx českou xxxxxxxxxx xxxxx, popřípadě xxxxxxxx xx xxxxxxx xxxxx xxxxxxxxx xxxxx, xxxx odkaz xx xxxx vyhlášku,
2. xxxxxxxxxxx x všech xxxxxxxxxx xxxxxxxxx x xxxxxxx xxxxxxxxxx, xxxxx xxxxx xxxxxxxx xxxxxxxx xxxxxxx,
3. xxxxx xxxxxx xxxxxx, xxxxxxxx xxxxx, xxxxxxx xxxx xxxxxxxxxx,
4. datum x xxx odběru xxxxxx,
5. xxxx odběru xxxxxx,
6. množství xxxxxx xxx laboratorní xxxxxxxx; xxxxx xxxx a xxxxxxxx v xxxxxx x xxxxxxxx potraviny, xxxxxxxx xxxx xxxxx x xxxxxxxx xxxxxxxxx,
7. xxxxx x podpis xxxxx, xxxxx xxxxxxxx xxxxx vzorku, x xxxxxx kontrolované xxxxx;
Xxxxxxxx
|
Xxxxxxxx xxxxx (x)
|
Xxxxxxxx nebo xxxxx xxxxx šarže
|
Počet xxxxxxx xxxxxx
|
Xxxxxxxx xxxxxxxxxx xxxxxx (xx)
|
Xxxxxxxxx a xxxxxxx x obilovin
|
≥ 1500
|
500 x
|
100
|
10
|
&xx; 300 x &xx; 1500
|
3 část xxxxx
|
100
|
10
|
|
≥ 50 a ≥ 300
|
100 t
|
100
|
10
|
|
< 50
|
-
|
3 xx 1001)
|
1 xx 10
|
|
Sušené hrozny xxxx xxxxx (korintky, xxxxxxx x xxxxxxxx)
|
≥ 15
|
15 xx b30 x
|
100
|
10
|
&xx; 15
|
-
|
10 xx 1002)
|
1 až 10
|
|
Xxxxxxx xxxxxx zrna, xxxxx xxxxxxx xxxx x xxxxxxxxx xxxx
|
≥ 15
|
15 xx 30 x
|
100
|
10
|
&xx; 15
|
-
|
10 až 1002)
|
1 xx 10
|
|
1) V xxxxxxxxxx xx hmotnosti xxxxx - xxx xxxxxxx 2 xxxx xxxxxxx.
|
||||
2) X xxxxxxxxxx xx xxxxxxxxx šarže - viz tabulka 3 xxxx xxxxxxx
|
Xxxxxxxx šarže (x)
|
Xxxxx xxxxxxx vzorků
|
≤ 0,05
|
3
|
&xx; 0,05 xx ≤ 0,5
|
5
|
&xx; 0,5 až ≤ 1
|
10
|
> 1 xx ≤ 3
|
20
|
> 3 xx ≤ 10
|
40
|
&xx; 10 xx ≤ 20
|
60
|
20 xx ≤ 50
|
100
|
Hmotnost šarže (x)
|
Xxxxx xxxxxxx xxxxxx
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≤ 0,1
|
10
|
&xx; 0,1 xx ≤ 0,2
|
15
|
> 0,2 xx ≤ 0,5
|
20
|
&xx; 0,5 xx ≤ 1,0
|
30
|
&xx; 1,0 xx ≤ 2,0
|
40
|
> 2,0 xx ≤ 5,0
|
60
|
&xx; 5,0 xx ≤ 10,0
|
80
|
&xx; 10,0 až ≤ 15,0
|
100
|
Xxxxx xxxxxxx xx xxx
|
Xxxxxxxx šarže xxxxxxxxx x&xxxx;xxxxxxxxxx xxxxxxxxxx (x)
|
Xxxxxxxxx xxxxx dílčích xxxxxx, xxxxx xxxx být xxxxxxxx
|
Xxxxx xxxxxx xxxxxxx (xxxxxxxx xxxxx, xxxx)
|
-
|
3
|
Xxxxx / balení hroznové xxxxx
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≤ 50
|
3
|
Láhve / xxxxxx xxxxxxxx xxxxx
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&xx; 50 xx 500
|
5
|
Láhve / xxxxxx xxxxxxxx xxxxx
|
&xx; 500
|
10
|
Láhve / xxxxxx xxxx
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≤ 50
|
1
|
Láhve / xxxxxx xxxx
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&xx; 50 xx 500
|
2
|
Xxxxx / balení xxxx
|
&xx; 500
|
3
|
Xxxxxxxx
|
Xxxxxxx TEF
|
Kongener
|
Hodnota XXX
|
Xxxxxxx-1,4-xxxxxxx (XXXX)
|
&xxxx; |
xxxxxxxxxxxxxx xxxxxxxx, polychlorované xxxxxxxx xxx xxxxx xxxxxx x&xxxx;xxxxxxxxxxxxx x xxxxxxxxxxxxxx xxxxxxxx s xxxxxx atomem chloru x xxxxxxxxxxx s xxxxxxxxxxx xxxxxxx
|
&xxxx; |
2,3,7,8-Xxxxxxxxxxxxxxxxxxxxxxx
|
1
|
xxxxxxxxxxxxxx xxxxxxxx xxx xxxxx xxxxxx x&xxxx;xxxxx-xxxxxxxx
|
|
1,2,3,7,8-Xxxxxxxxxxxxxxxxxxxxxxx
|
1
|
xxxxxxxxxxxxxx xxxxxxxx 77
|
0,0001
|
1,2,3,4,7,8-Xxxxxxxxxxxxxxxxxxxxxx
|
0,1
|
xxxxxxxxxxxxxx xxxxxxxx 81
|
0,0001
|
1,2,3,6,7,8- Xxxxxxxxxxxxxxxxxxxxxx
|
0,1
|
xxxxxxxxxxxxxx xxxxxxxx 126
|
0,1
|
1,2,3,7,8,9- Xxxxxxxxxxxxxxxxxxxxxx
|
0,1
|
xxxxxxxxxxxxxx xxxxxxxx 169
|
0,01
|
1,2,3,4,6,7,8-Xxxxxxxxxxxxxxxxxxxxxxx
|
0,01
|
&xxxx; | |
Xxxxxxxxxxxxxxxxxxxxxx
|
0,0001
|
&xxxx; | |
Xxxxxxxxxxxxx (PCDF)
|
|
polychlorované xxxxxxxx x&xxxx;xxxxxx atomem xxxxxx x&xxxx;xxxxx-xxxxxx
|
&xxxx; |
2,3,7,8-Xxxxxxxxxxxxxxxxxxxxxx
|
0,1
|
xxxxxxxxxxxxxx bifenyly 105
|
0,0001
|
1,2,3,7,8-Xxxxxxxxxxxxxxxxxxxxxx
|
0,05
|
xxxxxxxxxxxxxx xxxxxxxx 114
|
0,0005
|
2,3,4,7,8-Xxxxxxxxxxxxxxxxxxxxxx
|
0,5
|
xxxxxxxxxxxxxx xxxxxxxx 118
|
0,0001
|
1,2,3,4,7,8-Xxxxxxxxxxxxxxxxxxxxx
|
0,1
|
xxxxxxxxxxxxxx xxxxxxxx 123
|
0,0001
|
1,2,3,6,7,8-Xxxxxxxxxxxxxxxxxxxxx
|
0,1
|
xxxxxxxxxxxxxx xxxxxxxx 156
|
0,0005
|
1,2,3,7,8,9-Xxxxxxxxxxxxxxxxxxxxx
|
0,1
|
xxxxxxxxxxxxxx xxxxxxxx 157
|
0,0005
|
2,3,4,6,7,8-Hexachlordibenzofuran
|
0,1
|
polychlorované xxxxxxxx 167
|
0,00001
|
1,2,3,4,6,7,8-Xxxxxxxxxxxxxxxxxxxxxx
|
0,01
|
xxxxxxxxxxxxxx xxxxxxxx 189
|
0,0001
|
1,2,3,4,7,8,9-Heptachlordibenzofuran
|
0,01
|
|
|
Oktachlordibenzofuran
|
0,0001
|
||
*) xxxxx - Van xxx Berg xx xx. (1998) Toxic Xxxxxxxxxxx Factors (XXXx) xxx XXXx, PCDDs, XXXXx for Xxxxxx xxx xxx Xxxxxxxx. Xxxxxxxxxxxxx Health Perspectives, 106(12), 775.
|
Hmotnost šarže (xx)
|
Xxxxxxxxx xxxxx xxxxxxxxxx xxxxxxx xxxxxx
|
&xx; 50
|
3
|
50 xx 500
|
5
|
> 500
|
10
|
Xxxxx xxxxxx xxxx jednotek x šarži
|
Počet xxxxxxxxxx xxxxxx nebo xxxxxxxx
|
1 xx 25
|
1 xxxxxx xxxx xxxxxxxx
|
26 xx 100
|
xxx 5 %, xxxxxxx 2 xxxxxx xxxx xxxxxxxx
|
&xx; 100
|
xxx 5 %. xxxxxxxxx 10 xxxxxx xxxx xxxxxxxx
|
Xxxxxxxx xxxxx (xx)
|
Xxxxxxxxx xxxxx xxxxxxxxxx xxxxxxx vzorků
|
< 50
|
3
|
50 xx 500
|
5
|
&xx; 500
|
10
|
Xxxxx xxxxxx nebo jednotek x šarži
|
Počet xxxxxxxxxx xxxxxx xxxx xxxxxxxx
|
1 xx 25
|
1 balení xxxx xxxxxxxx
|
26 xx 100
|
xxx 5 %, xxxxxxx 2 xxxxxx xxxx xxxxxxxx
|
&xx; 100
|
asi 5 %, xxxxxxxxx 10 balení xxxx xxxxxxxx
|
Xxxxxxx x. 4 xxxxxxx právním xxxxxxxxx č. 611/2004 Sb.
Xxxxxxxx µx/x
|
Xxxxxxxxxx A
|
||
RSDr (%)
|
XXXX (%)
|
Xxxxxxxxx (%)
|
|
&xx; 1
|
≤ 40
|
≤ 60
|
50 xx 120
|
1 až 10
|
≤ 20
|
≤ 30
|
70 xx 110
|
Xxxxxxxxxxxxxxx
|
Xxxxxxx/xxxxxxxx
|
Xxxxxxxxxxxx
|
xxxxxxxxx xxxxxxx x xxxxxxxx Xxxxxxxxxx společenství č. 466/2001
|
Xxx xxxxxxx
|
xxxxx xxx xxxxx xxx jedna xxxxxxxx xxxxxxx xxxxxxx v xxxxxxxx Evropských xxxxxxxxxxxx č. 466/2001, xxxxx xxxxxxx, xxx xx pro xxxxx uvedena xxxxxxx xxxxx xxx 0,1 xx/xx. X tomto xxxxxxx xxxxx xxx xxxxx xxx xxxxx xxxxxx xxxxxxx hodnoty
|
Mez xxxxxxxxx
|
xxxxx xxx xxxxx xxx jedna xxxxxx xxxxxxx uvedené x xxxxxxxx Xxxxxxxxxx xxxxxxxxxxxx č. 466/2001, xxxxx xxxxxxx, xxx xx xxx xxxxx uvedena xxxxxxx xxxxx xxx 0,1 xx/xx. X tomto xxxxxxx xxxxx xxx xxxxx xxx xxx xxxxxx uvedené xxxxxxx
|
Xxxxxxxx
|
xxxxxxx XXXXXXx xxxx XXXXXXX x xxxxxxxxxxx xxxxxxxxx xxxxx xxxx xxx xxxxx xxx 1,5
|
Výtěžnost
|
80 - 120 % (xxxxx xxxxxxxxxxx kruhového xxxxx)
|
Xxxxxxxxxxxx
|
xxxxx xxxxx xxxxxxx xxxx xxxx xxxxx xxx spektrální xxxxxxx
|
Charakteristika
|
Doporučená hodnota
|
Koncentrace
|
Slepý xxxxx
|
Xxxxx xxx mez xxxxxxx
|
-
|
Xxxxxxx
|
75 xx 110 %
|
Xxxx xxxxxx koncentrací
|
Mez xxxxxxxxxxxxxxx
|
10 (xxxx méně) µx/xx, xxxxxxxx xx xxxxxx
|
-
|
Xxxxxxxxxx xxxxxxxx slepého xxxxxx
|
Xxxx xxx 4 µx/xx
|
-
|
Xxxxxx přesnosti x xxxxx xxxxxxxxxx - xxxxxxxxxx xxxxxxxx opakovaných xxxxxx xxx xxxxxxx xxxxxxxxxxxxx
|
&xx; 4 µg/kg
|
20 µx/xx
|
&xx; 6 µg/kg
|
30 µx/xx
|
|
&xx; 7 µx/xx
|
40 µx/xx
|
|
&xx; 8 µx/xx
|
50 µx/xx
|
|
&xx; 15 µx/xx
|
100 µx/xx
|
X(μx/xx)
|
α
|
≤ 50
|
0,2
|
51 - 100
|
0,18
|
501 - 1&xxxx;000
|
0,15
|
1&xxxx;001 - 10 000
|
0,12
|
≥ 10&xxxx;000
|
1
|
Xxxxxxxxxxxx xxxxxx
|
Xxxxxxxxxxx metody
|
|
Podíl falešně xxxxxxxxxxx xxxxxxxx
|
&xx; 1 %
|
-
|
Xxxxxxxxxx
|
-
|
-20 % až + 20 %
|
Xxxxxxxx xxxxxxxxxx
|
&xxxx;
&xx; 30%
|
< 15
|
Xxxxxxx x. 8 xxxxxxx xxxxxxx xxxxxxxxx č. 611/2004 Sb.
Příloha x. 9 xxxxxxx xxxxxxx xxxxxxxxx č. 611/2004 Sb.
Xxxxxxx x. 10 xxxxxxx právním xxxxxxxxx č. 611/2004 Sb.
(Metoda xxxxx výzkumného ústavu Xxxxxx Xxxxxxxx)
- x xxxxxxx xxxxx,
- x xxxxxxx xxxxx xxxxx,
- v xxxxxxx xxxxxxxxx xxxxx,
- v xxxxxxx xxxxx xxxxxxxxx xxxxx,
- x xxxxxx x xxxxxxxxxx cukru,
- x xxxxxx x xxxxxxxxxx xxxxx bílého.
- xx xxxxxxxxx xxxxxx,
- x xxxxxxx xxxxxxxxx xxxxxx.
- v glukosy xxxxxxxxxxx,
- x xxxxxxx xxxxxxx.
4.3.1. Xxxxxx síranu mědnatého: 25 x xxxxxxxxxxxx xxxxxx xxxxxxxxx xxxxxxxxxxxxxx xxxxxx xx xxxxxxxx xx 100 xx xxxx.
4.3.2. Roztok xxxxxxxx xxxxxxxxx: 50 g xxxxxxxxxxx xxxxxxxx xxxxxxxxx xx xxxxxxxx x 50 ml xxxx.
4.3.3. Xxxxxx xxxxxxxxxx xxxxxxx: 143,8 x bezvodého xxxxxxxxxx xxxxxxx xx xxxxxxxx x xxx 300 ml xxxxx xxxx a xxxxx xx vychladnout.
4.3.4. K xxxxxxx xxxxxxxxxx sodného (4.3.3.) v xxxxxxx xxxxxxx baňce xx xx mírného promíchávání xxxxxxxxx xxxxxxx přidává xxxxxx xxxxxxxx citronové (4.3.2.). Xxxxx xx xxxxx, xxxxx se xxxxxxxxxx xxxxxxx plyn, xxx xx xxxxx xxxxxx síranu mědnatého (4.3.1.) x xxxxx xx doplní xx 1000 xx. Roztok xx xxxxx xxxx xxxx noc, x xxxxxxx xxxxxxx xx xxxxx xxxxxxxxxxx. Xxxxxxx xx xxxxxxxx koncentrace xxxxxxx činidla xxxxx xxxxxx xxxxxxx x xxxx 6.1. (Xx 0,1 xxx/x; xxxxxxxxx xxxxx 1 mol/l).
6.1.1. Xx 25 xx Xxxx-Xxxxxxxxxx činidla (4.3.) xx přidají 3 x xxxxxx xxxxxxxxxx x 25 ml xxxxxxxx xxxxxx x xxxxxxxxxxx 3 xxx/x(4.6.).
6.1.2. Xxxxxxxxxx xx 10 ml činidla xx 100 xx xxxxxxx baňky a xxxxxx se vodou xx rysku.
6.1.3. 10 xx xxxxxxxxx činidla (6.1.2.) xx xxxxxxx xxxxxxxxx xxxxxxxxxxxxxxx, 0,1 mol/l (4.11.) za xxxxxxx xxxxxxxxxxxxx (4.12.) jako xxxxxxxxxx. Bod xxxxxxxxxxx xxx xxxxxxx xx xxxxxxxxxxxxxxx xxxxxxx xxxxxxxxx xxxxxxxx.
6.1.4. Xxxxxxx xX Xxxx-Xxxxxxxxxx xxxxxxx xxxx xxx mezi 9,3 a 9,4 xxx 20 °X.
6.2.1. Xxxxxx xx 5 x xxxxxx x xxxxxxxxx xx 1 xx x xxxxxxxxxxxxx se xxxxxxx xx xxxxxxx xxxxx x objemu 250 xx obsahující 200 xx xxxx. X xxxxxxx xxxxxxx xx vyčeří přidáním 5 ml Xxxxxxxxx xxxxxxx I (4.1.), xxx xx přidá 5 xx Xxxxxxxxx xxxxxxx XX (4.2.). Xx přídavku xxxxxxx xxxxxxx se xxxxx xxxxxxx. Xxxxxx xx xxxxxx xxxxx xx 250 xx x xxxxx xxxxxxxx. X xxxxxxx xxxxxxx xx xxxxxx xxxxxxxxxxx.
6.2.2. Xxxxxx (6.2.1.) xx xxxxx x takovém xxxxxx, xxx obsah xxxxxxxxxxxx xxxxx xxxxxxxxxxx jako xxxxxxx xx x 25 xx xxxxxxx xxxxxxxxx x xxxxxxx 15 xx 60 xx.
0,1 xxx/x thiosíranu xxxxxxx
|
Xxxxxxx, xxxxxxxx, inertní xxxx X6X1206
|
|
xx
|
xx
|
xxxxxx
|
1
|
2,4
|
&xxxx;
|
2
|
4,8
|
2,4
|
3
|
7,2
|
2,4
|
4
|
9,7
|
2,5
|
5
|
12,2
|
2,5
|
6
|
14,7
|
2,5
|
7
|
17,2
|
2,5
|
8
|
19,8
|
2,6
|
9
|
22,4
|
2,6
|
10
|
25,0
|
2,6
|
11
|
27,6
|
2,6
|
12
|
30,3
|
2,7
|
13
|
33,0
|
2,7
|
14
|
35,7
|
2,7
|
15
|
38,5
|
2,8
|
16
|
41,3
|
2,8
|
17
|
44,2
|
2,9
|
18
|
47,1
|
2,9
|
19
|
50,0
|
2,9
|
20
|
53,0
|
3,0
|
21
|
56,0
|
3,0
|
22
|
59,1
|
3,1
|
23
|
62,2
|
3,1
|
4.1.1. Roztok X:
4.1.2. Xxxxxx X:
6.1.1. Xx čisté x xxxxx xxxxxxx se xxxxxxxxxx 50 xx xxxxxxx X (4.1.2.), xxxx 50 ml xxxxxxx A (4.1.1.) x dobře xx xxxxxxxx.
6.1.2. Byreta xx xxxxxxxxxx x naplní 0,25 % (0,25 x/100 ml) standardním xxxxxxxx inverzního xxxxx (4.3.).
6.1.3. Xx 500 xx xxxxx xxxxx (5.1.) xx xxxxxxxxxx xxxxxxxxx xxxxx 20 xx xxxxxxxx xxxxxxx X a B (6.1.1.) a xxxxxxx xx 15 xx xxxx. Z xxxxxx xx do baňky xxxxxx 39 ml xxxxxxx xxxxxxxxxx xxxxx, xxxxx se xxxxxxx xxxxxxx kamínků a xxxxx xx xxxxxx xxxxxxxxx pohybem promíchá.
6.1.4. Xxxxx xxxxx se xxxxxxx x varu x nechá se xxxxx xx xxxx xxxxxx 2 xxx. Xxxxx xxxxxxx xxxxxxx xx xxxxx nesmí xxxxxxx xx zdroje xxxxx x xxxxxxxx xxx.
Xx konci xxxxxxxxxxxxxx xxxx xx přidají xxx xxxx xxxxx xxxxx xxxxxxx methylenové xxxxx (4.4.). Barva xxxxxxx musí být xxxxxxx xxxxx.
6.1.5. Xxxxxxxxx xx v xxxxxxxxx xxxxxxxxxxxx xxxxxxx xxxxxxxxxx xxxxx x xxxxxx, xxxxxxxx xx 0,2 xx, xxx xx 0,1 xx x xxxxxxx xx xxxxxxx, xx xx dosáhne xxxx ekvivalence. Ten xx xxxxxxxxx vymizením xxxxxxx zbarvení xxxxxxxx xxxxxxxxxxx xxxxx. Xxxxx xxxxxxx xx načervenalá xxxxxxxxx xxxxxxxxxxx xxxxxxxx xxxxx xxxxxxx.
6.1.6. Xxxx xxxxxxxxxxx při xxxxxxx xx mělo být xxxxxxxx xx xxx xxxxx xx xxxxxxx xxxx xxxxxxx. Xxxxxxx xxxxxxxx Vo xx xxxx xxxxxxxxx x xxxxxxx 39,0 xx 41,0 xx. Xx-xx xxxxxxx Vo xxxx xxxxxxx xxxxxx xxxxxxx, xxxxxx se xxxxxxxxxxx xxxx xx Xxxxxxxxxx xxxxxxx X (4.1.1.) x xxxxxxxxx titru xx opakuje.
6.3.1. Xx nutné provést xxxxxxxxxx zkoušku xx xxxxxxxx xxxxxxxxxx přídavku xxxx x 20 xx směsného xxxxxxx X x X, xxxxx zajistí, xx xxxxxxx objem xx xxxxxxx xxxx xxxxx 75 xx.
6.3.2. Xxxxx xx xxxxxxxx xxxxxxx xxxxxxxxxxx xxxxx xxxxxxxxx xxxxxxxxxxx xxxxxxxx, xx xxxxxxx xxxxxx xxxxxx příliš xxxxxxxxxxxxx. X xxxxx xxxxxxx se zkouška xxxxxxx x xxxxxxx xx opakované xxxxxxxxx x xxxxx koncentrací xxxxxxx xxxxxx.
6.4.1. Do xxxxx xxxxx se odpipetuje 20 xx xxxxxxxx Xxxxxxxxxx xxxxxxx a xxxxxxxx xxxx stanovené xxxxx xxxx 6.3.
6.4.2. X xxxxxx xx xxxxxx roztok vzorku x množství xxxxxxxxxx xxxxx xxxx 6.3., xxxxxxxx x 1 xx. Přidá se xxxxxxx varných xxxxxxx, xxxxx baňky se xxxxxxxxx pohybem xxxxxxxx, xxxxxx x xxxxxxx xxxx v xxxxxxxxxx xxxxxx (6.3.). Xxxx xxxxxxxxxxx při xxxxxxx xxxx být dosaženo xxxxx 1 xxx xx xxxxxxx xxxxxxx xxxxxxxxxxx xxxxx. Xxxxxxxx xxx xxxxxxx xxxxxxx xx xxxxx V1.
Xxxxxxxxx (x xx xxxxx )
|
Xxxxxxxx xxxxxx x
|
0,0
|
1,000
|
0,5
|
0,982
|
1,0
|
0,971
|
1,5
|
0,962
|
2,0
|
0,954
|
2,5
|
0,946
|
3,0
|
0,939
|
3,5
|
0,932
|
4,0
|
0,926
|
4,5
|
0,920
|
5,0
|
0,915
|
5,5
|
0,910
|
6,0
|
0,904
|
6,5
|
0,898
|
7,0
|
0,893
|
7,5
|
0,888
|
8,0
|
0,883
|
8,5
|
0,878
|
9,0
|
0,874
|
9,5
|
0,869
|
10,0
|
0,864
|
6.2.1. Xxxxxxxxxx xx nastaví xx xxxx.
6.2.2. Xxxxxx xx xxxxxxxxxxx přes filtrační xxxxx. Prvních 10 xx filtrátu se xxxxxxxxx, jímá se xx dalších 50 xx xxxxxxxx.
6.2.3. Polarometrická xxxxxxx xx promyje xxxxxxxxxxxx xxxxxxxxxxxxx xxxxxxxx xxxxxx xxxxxxxx xx xxxxxxx (6.2.2.).
6.2.4. Xxxxxxx xx xxx xxxxxxx (20 ± 0,1)° X opatrně xxxxxx xxxxxxxx xxxxxx xxxxxxxx xx xxxxxxx.
Xxx xxxxxxxxx xxxxxxxxx xxxxxxxx xx xxxxxxxx xxxxxxx xxxxxxxxx xxxxxxx. Xxxxxxxx xxxxxxx xx xxxxxx xx xxxxxxx xxxxxxxxx.
6.2.5. Xxxxxx xx polarizace x xxxxxxxxx xx 0,05 °X nebo 0,02 xxxxxxxx xxxxxx. Xxxxx xx xxxxxxxx xxxxx xxxxxxxxx. Vypočte xx xxxxxx x xxxxxx xxxx xxxxxx.
2.1.1. Xxxxxxx xx xxxxxxx xxxx xxx xxxxxxx, xxxxxx xxxx xxxxxxxxx, xxxx xx xxxxxxxxxxx xxxx xxxx xxxxxxxxxxxxxxxx voda xxxxxxx xxxxxxxxxxxx xxxxxxx.
2.1.2. Xxxxxxx je zmínka x roztoku xxxx xxxxxx, aniž xx xxxxxx xxxxx xxxx, xxxx xx xxxxx xxxxxx.
6.1.1. X přesností xx 1 xx se xxxxxx 0,1 x xxxxxx x xxxxxxxx xx v 10 xx 95% xxxxxxxx (4.2). Xxxxxx xx xxxxxxx xx xxxxxxxxx Xxxxxxxxxx xxxxx (5.1) x zředí se xxxxx na 50 xx. Zamíchá xx x xx míchání xx přidá 1 x xxxxxx amonno-železitého (4.1). Nechá se xxxxxx stát.
6.1.2. Xxxxxxxx xx zopakováním xxxxxxx 6.1.1 xxxxxxxx srovnávací xxxxxx, xxx 0,1 x vzorku xx xxxxxxx 1 xx xxxxxxx xxxxxxxx xxxxxxxxxx (4.3).
6.1.3. Xxxxxxxxx xxxxxxx xxxxxx xx xxxxxxx xx xxxxxxxxxx xxxxxxxxxxxx xxxxxxx.
6.2.1. Xxxxxxxx xx postup 6.1.1, xxxx xxxxxxxx xx 50 xx xx xxxxxxx xxxxxxxxx xxxxxxxxx xxxxxxx (4.4) o xxxxxxxxxxx 1 xxx/x xx xX 5.
6.2.2. Xxxxxxxx xx xxxxxx 6.1.2.
6.2.3. Xxxxxxxx se xxxxxx 6.1.3.
5.2.1. 100xx xxxxxxxxx xxxxx x kulatým xxxx;
5.2.2. xxxxxxxx xxxxxxxx;
5.2.3. xxxxxxxx xxxxxxx, 250 xx xxxxxx x xxxxxxxx xxxxxxxx 22 mm, xx zábrusem; xxxxxxxxxxxx x xxxxxxxx rozměrech - xxxxxx 20 xx x výška 35 xx 50 xx.
![](https://objekty.epis.cz/files/21104_02.gif)
![](https://objekty.epis.cz/files/21104_03.gif)
6.3.1. Xxxxxxxx xxxx důkazů xxxxxxxxxxxx xxxxxxxx prováděných xxxxxxxx xxxx xxxxxx xx xxxx ve xxxxxxx xxxxxx a xxxxxxx xxxxxxxxxxx xx xxxxxxxx xxxxxxxx xxxx xxx xxxxxx.
6.3.2. Xxx Xxxxxxxxxx xxxxxxx reagují x xxxxxxx, xx xxxx xx vzorku xxxxxxxx 2 % xxxxxxx.
6.2.1. Xxxxxxx xx xxxxx xxxxx.
6.2.2. Xxxxxxxx xxxx xxxxxx xxxxxxxxxxxx xxxxxxxx prováděných xxxxxxxx xxxx xxxxxx po xxxx xx xxxxxxx xxxxxx x xxxxxxx xxxxxxxxxxx za xxxxxxxx xxxxxxxx musí xxx xxxxxx.
6.2.3. Xxxxxx xxxxxxxxxxxxx xxxxxx xxx 60 xxx xx se xxxxx xxxxxxxx.
6.2.4. Pokud xx xxxxx pozitivní xxxxxxxx, xxxx xxxxxx xxxxxxxxx xxxxxxxxx x xxxxx xxxxxxxxx xxxxx x zkouška xxxx xxx xxxxxxxxxx xxxxx xxxxxx ISO 3709 (1976) "Kyselina xxxxxxxxxx xxx xxxxxxxxxx použití (xxxxxx potravin) - xxxxxxxxx xxxxxx xxxxx xxxxxx xxxxxxxxxxxxxxxxxxxx metodou x 3,4-xxxxxxxxx".
4.1.1. Xxxxxxx xxxxxx, xxxxx xx xxx 20 °X pH 6,88, xx xxxxxx ze xxxxxxxx objemů xxxxxxx xxxxxxxxxxxxxxxxxxxxxx xxxxxxxxxx o xxxxxxxxxxx 0,05 mol/l x xxxxxxxxxxxxxxxxxxxx xxxxxxx x xxxxxxxxxxx 0,05 xxx/X.
4.1.2. Tlumivý roztok, xxxxx xx xxx 20 °C xX 4, xx roztok xxxxxxxxxxxxxxx draselného x xxxxxxxxxxx 0,05 xxx/x.
4.1.3. Xxxxxxx xxxxxx, xxxxx xx při 20 °X xX 9, xx xxxxxx xxxxxxx xxxxxxxx sodného x xxxxxxxxxxx 0,05 mol/l.
°X) |
Xxxxxxxxx (%) |
x (20 °X) |
Xxxxxxxxx (%) |
n (20 °X) |
Xxxxxxxxx (%) |
x (20 °X) |
Xxxxxxxxx (%) |
n (20 °X) |
Xxxxxxxxx (%) |
1,3330 |
0,009 |
1,3365 |
2,436 |
1,3400 |
4,821 |
1,3435 |
7,164 |
1,3470 |
9,466 |
1,3331 |
0,078 |
1,3366 |
2,505 |
1,3401 |
4,888 |
1,3436 |
7,230 |
1,3471 |
9,531 |
1,3332 |
0,149 |
1,3367 |
2,574 |
1,3402 |
4,956 |
1,3437 |
7,296 |
1,3472 |
9,596 |
1,3333 |
0,218 |
1,3368 |
2,642 |
1,3403 |
5,023 |
1,3438 |
7,362 |
1,3473 |
9,661 |
1,3334 |
0,288 |
1,3369 |
2,711 |
1,3404 |
5,091 |
1,3439 |
7,429 |
1,3474 |
9,726 |
1,3335 |
0,358 |
1,3370 |
2,779 |
1,3405 |
5,158 |
1,3440 |
7,495 |
1,3475 |
9,791 |
1,3336 |
0,428 |
1,3371 |
2,848 |
1,3406 |
5,225 |
1,3441 |
7,561 |
1,3476 |
9,856 |
1,3337 |
0,498 |
1,3372 |
2,917 |
1,3407 |
5,293 |
1,3442 |
7,627 |
1,3477 |
9,921 |
1,3338 |
0,567 |
1,3373 |
2,985 |
1,3408 |
5,360 |
1,3443 |
7,693 |
1,3478 |
9,986 |
1,3339 |
0,637 |
1,3374 |
3,053 |
1,3409 |
5,427 |
1,3444 |
7,759 |
1,3479 |
10,051 |
1,3340 |
0,707 |
1,3375 |
3,122 |
1,3410 |
5,494 |
1,3445 |
7,825 |
1,3480 |
10,116 |
1,3341 |
0,776 |
1,3376 |
3,190 |
1,3411 |
5,562 |
1,3446 |
7,891 |
1,3481 |
10,181 |
1,3342 |
0,846 |
1,3377 |
3,259 |
1,3412 |
5,629 |
1,3447 |
7,957 |
1,3482 |
10,246 |
1,3343 |
0,915 |
1,3378 |
3,327 |
1,3413 |
5,696 |
1,3448 |
8,023 |
1,3483 |
10,311 |
1,3344 |
0,985 |
1,3379 |
3,395 |
1,3414 |
5,763 |
1,3449 |
8,089 |
13,484 |
10,375 |
1,3345 |
1,054 |
1,3380 |
3,463 |
1,3415 |
5,830 |
1,3450 |
8,155 |
1,3485 |
10,440 |
1,3346 |
1,124 |
1,3381 |
3,532 |
1,3416 |
5,897 |
1,3451 |
8,221 |
1,3486 |
10,505 |
1,3347 |
1,193 |
1,3382 |
3,600 |
1,3417 |
5,964 |
1,3452 |
8,287 |
1,3487 |
10,570 |
1,3348 |
1,263 |
1,3383 |
3,668 |
1,3418 |
6,031 |
1,3453 |
8,352 |
1,3488 |
10,634 |
1,3349 |
1,332 |
1,3384 |
3,736 |
1,3419 |
6,098 |
1,3454 |
8,418 |
1,3489 |
10,699 |
1,3350 |
1,401 |
1,3385 |
3,804 |
1,3420 |
6,165 |
1,3455 |
8,484 |
1,3490 |
10,763 |
1,3351 |
1,470 |
1,3386 |
3,872 |
1,3421 |
6,231 |
1,3456 |
8,550 |
1,3491 |
10,828 |
1,3352 |
1,540 |
1,3387 |
3,940 |
1,3422 |
6,298 |
1,3457 |
8,615 |
1,3492 |
10,892 |
1,3353 |
1,609 |
1,3388 |
4,008 |
1,3423 |
6,365 |
1,3458 |
8,681 |
1,3493 |
10,957 |
1,3354 |
1,678 |
1,3389 |
4,076 |
1,3424 |
6,432 |
1,3459 |
8,746 |
1,3494 |
11,021 |
1,3355 |
1,747 |
1,3390 |
4,144 |
1,3425 |
6,498 |
1,3460 |
8,812 |
1,3495 |
11,086 |
1,3356 |
1,816 |
1,3391 |
4,212 |
1,3426 |
6,565 |
1,3461 |
8,878 |
1,3496 |
11,150 |
1,3357 |
1,885 |
1,3392 |
4,279 |
1,3427 |
6,632 |
1,3462 |
8,943 |
1,3497 |
11,215 |
1,3358 |
1,954 |
1,3393 |
4,347 |
1,3428 |
6,698 |
1,3463 |
9,008 |
1,3498 |
11,279 |
1,3359 |
2,023 |
1,3394 |
4,415 |
1,3429 |
6,765 |
1,3464 |
9,074 |
1,3499 |
11,343 |
1,3360 |
2,092 |
1,3395 |
4,483 |
1,3430 |
6,831 |
1,3465 |
9,139 |
1,3500 |
11,407 |
1,3361 |
2,161 |
1,3396 |
4,550 |
1,3431 |
6,898 |
1,3466 |
9,205 |
1,3501 |
11,472 |
1,3362 |
2,230 |
1,3397 |
4,618 |
1,3432 |
6,964 |
1,3467 |
9,270 |
1,3502 |
11,536 |
3363 |
2,299 |
1,3398 |
4,686 |
1,3433 |
7,031 |
1,3468 |
9,335 |
1,3503 |
11,600 |
1,3364 |
2,367 |
1,3399 |
4,753 |
1,3434 |
7,097 |
1,3469 |
9,400 |
1,3504 |
11,664 |
1,3505 |
11,728 |
1,3560 |
15,207 |
1,3615 |
18,595 |
1,3670 |
21,896 |
1,3725 |
25,114 |
1,3506 |
11,792 |
1,3561 |
15,269 |
1,3616 |
18,655 |
1,3671 |
21,955 |
1,3726 |
25,172 |
1,3507 |
11,856 |
1,3562 |
15,332 |
1,3617 |
18,716 |
1,3672 |
22,014 |
1,3727 |
25,230 |
1,3508 |
11,920 |
1,3563 |
15,394 |
1,3618 |
18,777 |
1,3673 |
22,073 |
1,3728 |
25,287 |
1,3509 |
11,984 |
1,3564 |
15,456 |
1,3619 |
18,837 |
1,3674 |
22,132 |
1,3729 |
25,345 |
1,3510 |
12,048 |
1,3565 |
15,518 |
1,3620 |
18,898 |
1,3675 |
22,192 |
1,3730 |
25,403 |
1,3511 |
12,112 |
1,3566 |
15,581 |
1,3621 |
18,959 |
1,3676 |
22,251 |
1,3731 |
25,460 |
1,3512 |
12,176 |
1,3567 |
15,643 |
1,3622 |
19,019 |
1,3677 |
22,310 |
1,3732 |
25,518 |
1,3513 |
12,240 |
1,3568 |
15,705 |
1,3623 |
19,080 |
1,3678 |
22,369 |
1,3733 |
25,576 |
1,3514 |
12,304 |
1,3569 |
15,767 |
1,3624 |
19,141 |
1,3679 |
22,428 |
1,3734 |
25,633 |
1,3515 |
12,368 |
1,3570 |
15,829 |
1,3625 |
19,201 |
1,3680 |
22,487 |
1,3735 |
25,691 |
1,3516 |
12,431 |
1,3571 |
15,891 |
1,3626 |
19,262 |
1,3681 |
22,546 |
1,3736 |
25,748 |
1,3517 |
12,495 |
1,3572 |
15,953 |
1,3627 |
19,322 |
1,3682 |
22,605 |
1,3737 |
25,806 |
1,3518 |
12,559 |
1,3573 |
16,016 |
1,3628 |
19,382 |
1,3683 |
22,664 |
1,3738 |
25,863 |
1,3519 |
12,623 |
1,3574 |
16,078 |
1,3629 |
19,443 |
1,3684 |
22,723 |
1,3739 |
25,921 |
1,3520 |
12,686 |
1,3575 |
16,140 |
1,3630 |
19,503 |
1,3685 |
22,781 |
1,3740 |
25,978 |
1,3521 |
12,750 |
1,3576 |
16,201 |
1,3631 |
19,564 |
1,3686 |
22,840 |
1,3741 |
26,035 |
1,3522 |
12,813 |
1,3577 |
16,263 |
1,3632 |
19,624 |
1,3687 |
22,899 |
1,3742 |
26,093 |
1,3523 |
12,877 |
1,3578 |
16,325 |
1,3633 |
19,684 |
1,3688 |
22,958 |
1,3743 |
26,150 |
1,3524 |
12,940 |
1,3579 |
16,387 |
1,3634 |
19,745 |
1,3689 |
23,017 |
1,3744 |
26,207 |
1,3525 |
13,004 |
1,3580 |
16,449, |
1,3635 |
19,805 |
1,3690 |
23,075 |
1,3745 |
26,265 |
1,3526 |
13,067 |
1,3581 |
16,511 |
1,3636 |
19,865 |
1,3691 |
23,134 |
1,3746 |
26,322 |
1,3527 |
13,131 |
1,3582 |
16,573 |
1,3637 |
19,925 |
1,3692 |
23,193 |
1,3747 |
26,379 |
1,3528 |
13,194 |
1,3583 |
16,634 |
1,3638 |
19,985 |
1,3693 |
23,251 |
1,3748 |
26,436 |
1,3529 |
13,258 |
1,3584 |
16,696 |
1,3639 |
20,045 |
1,3694 |
23,310 |
1,3749 |
26,493 |
1,3530 |
13,321 |
1,3585 |
16,758 |
1,3640 |
20,106 |
1,3695 |
23,369 |
1,3750 |
26,551 |
1,3531 |
13,384 |
1,3586 |
16,819 |
1,3641 |
20,166 |
1,3696 |
23,427 |
1,3751 |
26,608 |
1,3532 |
13,448 |
1,3587 |
16,881 |
1,3642 |
20,226 |
1,3697 |
23,486 |
1,3752 |
26,665 |
1,3533 |
13,511 |
1,3588 |
16,943 |
1,3643 |
20,286 |
1,3698 |
23,544 |
1,3753 |
26,722 |
1,3534 |
13,574 |
1,3589 |
17,004 |
1,3644 |
20,346 |
1,3699 |
23,603 |
1,3754 |
26,779 |
1,3535 |
13,637 |
1,3590 |
17,066 |
1,3645 |
20,406 |
1,3700 |
23,661 |
1,3755 |
26,836 |
1,3536 |
13,700 |
1,3591 |
17,127 |
1,3646 |
20,466 |
1,3701 |
23,720 |
1,3756 |
26,893 |
1,3537 |
13,763 |
1,3592 |
17,189 |
1,3647 |
20,525 |
1,3702 |
23,778 |
1,3757 |
26,950 |
1,3538 |
13,826 |
1,3593 |
17,250 |
1,3648 |
20,585 |
1,3703 |
23,836 |
1,3758 |
27,007 |
1,3539 |
13,890 |
1,3594 |
17,311 |
1,3649 |
20,645 |
1,3704 |
23,895 |
1,3759 |
27,064 |
1,3540 |
13,953 |
1,3595 |
17,373 |
1,3650 |
20,705 |
1,3705 |
23,953 |
1,3760 |
27,121 |
1,3541 |
14,016 |
1,3596 |
17,434 |
1,3651 |
20,765 |
1,3706 |
24,011 |
1,3761 |
27,178 |
1,3542 |
14,079 |
1,3597 |
17,496 |
1,3652 |
20,825 |
1,3707 |
24,070 |
1,3762 |
27,234 |
1,3543 |
14,141 |
1,3598 |
17,557 |
1,3653 |
20,884 |
1,3708 |
24,128 |
1,3763 |
27,291 |
1,3544 |
14,204 |
1,3599 |
17,618 |
1,3654 |
20,944 |
1,3709 |
24,186 |
1,3764 |
27,348 |
1,3545 |
14,267 |
1,3600 |
17,679 |
1,3655 |
21,004 |
1,3710 |
24,244 |
1,3765 |
27,405 |
1,3546 |
14,330 |
1,3601 |
17,741 |
1,3656 |
21,063 |
1,3711 |
24,302 |
1,3766 |
27,462 |
1,3547 |
14,393 |
1,3602 |
17,802 |
1,3657 |
21,123 |
1,3712 |
24,361 |
1,3767 |
27,518 |
1,3548 |
14,456 |
1,3603 |
17,863 |
1,3658 |
21,183 |
1,3713 |
24,419 |
1,3768 |
27,575 |
1,3549 |
14,518 |
1,3604 |
17,924 |
1,3659 |
21,242 |
1,3714 |
24,477 |
1,3769 |
27,632 |
1,3550 |
14,581 |
1,3605 |
17,985 |
1,3660 |
21,302 |
1,3715 |
24,535 |
1,3770 |
27,688 |
1,3551 |
14,644 |
1,3606 |
18,046 |
1,3661 |
21,361 |
1,3716 |
24,593 |
1,3771 |
27,745 |
1,3552 |
14,707 |
1,3607 |
18,107 |
1,3662 |
21,421 |
1,3717 |
24,651 |
1,3772 |
27,802 |
1,3553 |
14,769 |
1,3608 |
18,168 |
1,3663 |
21,480 |
1,3718 |
24,709 |
1,3773 |
27,858 |
1,3554 |
14,832 |
1,3609 |
18,229 |
1,3664 |
21,540 |
1,3719 |
24,767 |
1,3774 |
27,915 |
1,3555 |
14,894 |
1,3610 |
18,290 |
1,3665 |
21,599 |
1,3720 |
24,825 |
1,3775 |
27,971 |
1,3556 |
14,957 |
1,3611 |
18,351 |
1,3666 |
21,658 |
1,3721 |
24,883 |
1,3776 |
28,028 |
1,3557 |
15,019 |
1,3612 |
18,412 |
1,3667 |
21,718 |
1,3722 |
24,941 |
1,3777 |
28,084 |
1,3558 |
15,082 |
1,3613 |
18,473 |
1,3668 |
21,777 |
1,3723 |
24,998 |
1,3778 |
28,141 |
1,3559 |
15,144 |
1,3614 |
18,534 |
1,3669 |
21,836 |
1,3724 |
25,056 |
1,3779 |
28,197 |
1,3780 |
28,253 |
1,3835 |
31,317 |
1,3890 |
34,310 |
1,3945 |
37,233 |
1,4000 |
40,091 |
1,3781 |
28,310 |
1,3836 |
31,372 |
1,3891 |
34,363 |
1,3946 |
37,286 |
1,4001 |
40,142 |
1,3782 |
28,366 |
1,3837 |
31,428 |
1,3892 |
34,417 |
1,3947 |
37,338 |
1,4002 |
40,194 |
1,3783 |
28,422 |
1,3838 |
31,482 |
1,3893 |
34,471 |
1,3948 |
37,391 |
1,4003 |
40,245 |
1,3784 |
28,479 |
1,3839 |
31,537 |
1,3894 |
34,524 |
1,3949 |
37,443 |
1,4004 |
40,296 |
1,3785 |
28,535 |
1,3840 |
31,592 |
1,3895 |
34,578 |
1,3950 |
37,495 |
1,4005 |
40,348 |
1,3786 |
28,591 |
1,3841 |
31,647 |
1,3896 |
34,632 |
1,3951 |
37,548 |
1,4006 |
40,399 |
1,3787 |
28,648 |
1,3842 |
31,702 |
1,3897 |
34,685 |
1,3952 |
37,600 |
1,4007 |
40,450 |
1,3788 |
28,704 |
1,3843 |
31,757 |
1,3898 |
34,739 |
1,3953 |
37,653 |
1,4008 |
40,501 |
1,3789 |
28,760 |
1,3844 |
31,812 |
1,3899 |
34,793 |
1,3954 |
37,705 |
1,4009 |
40,553 |
1,3790 |
28,816 |
1,3845 |
31,867 |
1,3900 |
34,846 |
1,3955 |
37,757 |
1,4010 |
40,604 |
1,3791 |
28,872 |
1,3846 |
31,922 |
1,3901 |
34,900 |
1,3956 |
37,810 |
1,4011 |
40,655 |
1,3792 |
28,928 |
1,3847 |
31,976 |
1,3902 |
34,953 |
1,3957 |
37,862 |
1,4012 |
40,706 |
1,3793 |
28,984 |
1,3848 |
32,031 |
1,3903 |
35,007 |
1,3958 |
37,914 |
1,4013 |
40,757 |
1,3794 |
29,040 |
1,3849 |
32,086 |
1,3904 |
35,060 |
1,3959 |
37,967 |
1,4014 |
40,808 |
1,3795 |
29,096 |
1,3850 |
32,140 |
1,3905 |
35,114 |
1,3960 |
38,019 |
1,4015 |
40,860 |
1,3796 |
29,152 |
1,3851 |
32,195 |
1,3906 |
35,167 |
1,3961 |
38,071 |
1,4016 |
40,911 |
1,3797 |
29,208 |
1,3852 |
32,250 |
1,3907 |
35,220 |
1,3962 |
38,123 |
1,4017 |
40,962 |
1,3798 |
29,264 |
1,3853 |
32,304 |
1,3908 |
35,274 |
1,3963 |
38,175 |
1,4018 |
41,013 |
1,3799 |
29,320 |
1,3854 |
32,359 |
1,3909 |
35,327 |
1,3964 |
38,228 |
1,4019 |
41,064 |
1,3800 |
29,376 |
1,3855 |
32,414 |
1,3910 |
35,380 |
1,3965 |
38,280 |
1,4020 |
41,115 |
1,3801 |
29,432 |
1,3856 |
32,468 |
1,3911 |
35,434 |
1,3966 |
38,332 |
1,4021 |
41,166 |
1,3802 |
29,488 |
1,3857 |
32,523 |
1,3912 |
35,487 |
1,3967 |
38,384 |
1,4022 |
41,217 |
1,3803 |
29,544 |
1,3858 |
32,577 |
1,3913 |
35,540 |
1,3968 |
38,436 |
1,4023 |
41,268 |
1,3804 |
29,600 |
1,3859 |
32,632 |
1,3914 |
35,593 |
1,3969 |
38,488 |
1,4024 |
41,318 |
1,3805 |
29,655 |
1,3860 |
32,686 |
1,3915 |
35,647 |
1,3970 |
38,540 |
1,4025 |
41,369 |
1,3806 |
29,711 |
1,3861 |
32,741 |
1,3916 |
35,700 |
1,3971 |
38,592 |
1,4026 |
41,420 |
1,3807 |
29,767 |
1,3862 |
32,795 |
1,3917 |
35,753 |
1,3972 |
38,644 |
1,4027 |
41,471 |
1,3808 |
29,823 |
1,3863 |
32,849 |
1,3518 |
35,806 |
1,3973 |
38,696 |
1,4028 |
41,522 |
1,3809 |
29,878 |
1,3864 |
32,904 |
1,3919 |
35,859 |
1,3974 |
38,748 |
1,4029 |
41,573 |
1,3810 |
29,934 |
1,3865 |
32,958 |
1,3920 |
35,912 |
1,3975 |
38,800 |
1,4030 |
41,623 |
1,3811 |
29,989 |
1,3866 |
33,013 |
1,3921 |
35,966 |
1,3976 |
38,852 |
1,4031 |
41,674 |
1,3812 |
30,045 |
1,3867 |
33,067 |
1,3922 |
36,019 |
1,3977 |
38,904 |
1,4032 |
41,725 |
1,3813 |
30,101 |
1,3868 |
33,121 |
1,3923 |
36,072 |
1,3978 |
38,955 |
1,4033 |
41,776 |
1,3814 |
30,156 |
1,3869 |
33,175 |
1,3924 |
36,125 |
1,3979 |
39,007 |
1,4034 |
41,826 |
1,3815 |
30,212 |
1,3870 |
33,230 |
1,3925 |
36,178 |
1,3980 |
39,059 |
1,4035 |
41,877 |
1,3816 |
30,267 |
1,3871 |
33,284 |
1,3926 |
36,231 |
1,3981 |
39,111 |
1,4036 |
41,928 |
1,3817 |
30,323 |
1,3872 |
33,338 |
1,3927 |
36,284 |
1,3982 |
39,163 |
1,4037 |
41,978 |
1,3818 |
30,378 |
1,3873 |
33,392 |
1,3928 |
36,337 |
1,3983 |
39,214 |
1,4038 |
42,029 |
1,3819 |
30,434 |
1,3874 |
33,446 |
1,3929 |
36,389 |
1,3984 |
39,266 |
1,4039 |
42,080 |
1,3820 |
30,489 |
1,3875 |
33,500 |
1,3930 |
36,442 |
1,3985 |
39,318 |
1,4040 |
42,130 |
1,3821 |
30,544 |
1,3876 |
33,555 |
1,3931 |
36,495 |
1,3986 |
39,370 |
1,4041 |
42,181 |
1,3822 |
30,600 |
1,3877 |
33,609 |
1,3932 |
36,548 |
1,3987 |
39,421 |
1,4042 |
42,231 |
1,3823 |
30,655 |
1,3878 |
33,663 |
1,3933 |
36,601 |
1,3988 |
39,473 |
1,4043 |
42,282 |
1,3824 |
30,711 |
1,3879 |
33,717 |
1,3934 |
36,654 |
1,3989 |
39,525 |
1,4044 |
42,332 |
1,3825 |
30,766 |
1,3880 |
33,771 |
1,3935 |
36,706 |
1,3990 |
39,576 |
1,4045 |
42,383 |
1,3826 |
30,821 |
1,3881 |
33,825 |
1,3936 |
36,759 |
1,3991 |
39,628 |
1,4046 |
42,433 |
1,3827 |
30,876 |
1,3882 |
33,879 |
1,3937 |
36,812 |
1,3992 |
39,679 |
1,4047 |
42,484 |
1,3828 |
30,932 |
1,3883 |
33,933 |
1,3938 |
36,865 |
1,3993 |
39,731 |
1,4048 |
42,534 |
1,3829 |
30,987 |
1,3884 |
33,987 |
1,3939 |
36,917 |
1,3994 |
39,782 |
1,4049 |
42,585 |
1,3830 |
31,042 |
1,3885 |
34,040 |
1,3940 |
36,970 |
1,3995 |
39,834 |
1,4050 |
42,635 |
1,3831 |
31,097 |
1,3886 |
34,094 |
1,3941 |
37,023 |
1,3996 |
39,885 |
1,4051 |
42,685 |
1,3832 |
31,152 |
1,3887 |
34,148 |
1,3942 |
37,075 |
1,3997 |
39,937 |
1,4052 |
42,736 |
1,3833 |
31,207 |
1,3888 |
34,202 |
1,3943 |
37,128 |
1,3998 |
39,988 |
1,4053 |
42,786 |
1,3834 |
31,262 |
1,3889 |
34,256 |
1,3944 |
37,180 |
1,3999 |
40,040 |
1,4054 |
42,836 |
1,4055 |
42,887 |
1,4110 |
45,623 |
1,4165 |
48,302 |
1,4220 |
50,928 |
1,4275 |
53,501 |
1,4056 |
42,937 |
1,4111 |
45,672 |
1,4166 |
48,350 |
1,4221 |
50,951 |
1,4276 |
53,548 |
1,4057 |
42,987 |
1,4112 |
45,721 |
1,4167 |
48,399 |
1,4222 |
51,022 |
1,4277 |
53,594 |
1,4058 |
43,037 |
1,4113 |
45,770 |
1,4168 |
48,447 |
1,4223 |
51,069 |
1,4278 |
53,640 |
1,1059 |
43,088 |
1,4114 |
45,820 |
1,4169 |
48,495 |
1,4224 |
51,116 |
1,4279 |
53,686 |
1,4060 |
43,138 |
1,4115 |
45,869 |
1,4170 |
48,543 |
1,4225 |
51,164 |
1,4280 |
53,733 |
1,4061 |
43,188 |
1,4116 |
45,918 |
1,4171 |
48,591 |
1,4226 |
51,211 |
1,4281 |
53,779 |
1,4062 |
43,238 |
1,4117 |
46,967 |
1,4172 |
48,639 |
1,4227 |
51,258 |
1,4282 |
53,825 |
1,4063 |
43,288 |
1,4118 |
46,016 |
1,4173 |
48,687 |
1,4228 |
51,305 |
1,4283 |
53,871 |
1,4064 |
43,338 |
1,4119 |
46,065 |
1,4174 |
48,735 |
1,4229 |
51,352 |
1,4284 |
53,918 |
1,4065 |
43,388 |
1,4120 |
46,114 |
1,4175 |
48,784 |
1,4230 |
51,399 |
1,4285 |
53,964 |
1,4066 |
43,439 |
1,4121 |
46,163 |
1,4176 |
48,832 |
1,4231 |
51,446 |
1,4286 |
54,010 |
1,4067 |
43,489 |
1,4122 |
46,212 |
1,4177 |
48,880 |
1,4232 |
51,493 |
1,4287 |
54,056 |
1,4068 |
43,539 |
1,4123 |
46,261 |
1,4178 |
48,928 |
1,4233 |
51,540 |
1,4288 |
54,102 |
1,4069 |
43,589 |
1,4124 |
46,310 |
1,4179 |
48,976 |
1,4234 |
51,587 |
1,4289 |
54,148 |
1,4070 |
43,639 |
1,4125 |
46,359 |
1,4180 |
49,023 |
1,4235 |
51,634 |
1,4290 |
54,194 |
1,4071 |
43,689 |
1,4126 |
46,408 |
1,4181 |
49,071 |
1,4236 |
51,681 |
1,4291 |
54,241 |
1,4072 |
43,739 |
1,4127 |
46,457 |
1,4182 |
49,119 |
1,4237 |
51,728, |
1,4292 |
54,287 |
1,4073 |
43,789 |
1,4128 |
46,506 |
1,4183 |
49,167 |
1,4238 |
51,775 |
1,4293 |
54,333 |
1,4074 |
43,838 |
1,4229 |
46,555 |
1,4184 |
49,215 |
1,4239 |
51,822 |
1,4294 |
54,379 |
1,4075 |
43,888 |
1,4130 |
46,604 |
1,4185 |
49,263 |
1,4240 |
51,869 |
1,4295 |
54,425 |
1,4076 |
43,938 |
1,4131 |
46,652 |
1,4186 |
49,311 |
1,4241 |
51,916 |
1,4296 |
54,471 |
1,4077 |
43,988 |
1,4132 |
46,701 |
1,4187 |
49,359 |
1,4242 |
51,963 |
1,4297 |
54,517 |
1,4078 |
44,038 |
1,4133 |
46,750 |
1,4188 |
49,407 |
1,4243 |
52,010 |
1,4298 |
54,563 |
1,4079 |
44,088 |
1,4134 |
46,799 |
1,4189 |
49,454 |
1,4244 |
52,057 |
1,4299 |
54,609 |
1,4080 |
44,138 |
1,4135 |
46,848 |
1,4190 |
49,502 |
1,4245 |
52,104 |
1,4300 |
54,655 |
1,4081 |
44,187 |
1,4136 |
46,896 |
1,4191 |
49,550 |
1,4246 |
52,150 |
1,4301 |
54,701 |
1,4082 |
44,237 |
1,4137 |
46,945 |
1,4192 |
49,598 |
1,4247 |
52,197 |
1,4302 |
54,746 |
1,4083 |
44,287 |
1,4138 |
46,994 |
1,4193 |
49,645 |
1,4248 |
52,244 |
1,4303 |
54,792 |
1,4084 |
44,337 |
1,4139 |
47,043 |
1,4194 |
49,693 |
1,4249 |
52,291 |
1,4304 |
54,838 |
1,4085 |
44,386 |
1,4140 |
47,091 |
1,4195 |
49,741 |
1,4250 |
52,338 |
1,4305 |
54,884 |
1,4086 |
44,436 |
1,4141 |
47,140 |
1,4196 |
49,788 |
1,4251 |
52,384 |
1,4306 |
54,930 |
1,4087 |
44,486 |
1,4142 |
47,188 |
1,4197 |
49,836 |
1,4252 |
52,431 |
1,4307 |
54,976 |
1,4088 |
44,535 |
1,4143 |
47,237 |
1,4198 |
49,884 |
1,4253 |
52,478 |
1,4308 |
55,022 |
1,4089 |
44,585 |
1,4144 |
47,286 |
1,4199 |
49,931 |
1,4254 |
52,524 |
1,4309 |
55,067 |
1,4090 |
44,635 |
1,4145 |
47,334 |
1,4200 |
49,979 |
1,4255 |
52,571 |
1,4310 |
55,113 |
1,4091 |
44,684 |
1,4146 |
47,383 |
1,4201 |
50,027 |
1,4256 |
52,618 |
1,4311 |
55,159 |
1,4092 |
44,734 |
1,4147 |
47,431 |
1,4202 |
50,074 |
1,4257 |
52,664 |
1,4312 |
55,205 |
1,4093 |
44,783 |
1,4148 |
47,480 |
1,4203 |
50,122 |
1,4258 |
52,711 |
1,4313 |
55,250 |
1,4094 |
44,833 |
1,4149 |
47,528 |
1,4204 |
50,169 |
1,4259 |
52,758 |
1,4314 |
55,296 |
1,4095 |
44,882 |
1,4150 |
47,577 |
1,4205 |
50,217 |
1,4260 |
52,804 |
1,4315 |
55,342 |
1,4096 |
44,932 |
1,4151 |
47,625 |
1,4206 |
50,264 |
1,4261 |
52,851 |
1,4316 |
55,388 |
1,4097 |
44,981 |
1,4152 |
47,674 |
1,4207 |
50,312 |
1,4262 |
52,897 |
1,4317 |
55,433 |
1,4098 |
45,031 |
1,4153 |
47,722 |
1,4208 |
50,359 |
1,4263 |
52,944 |
1,4318 |
55,479 |
1,4099 |
45,080 |
1,4154 |
47,771 |
1,4209 |
50,407 |
1,4264 |
52,990 |
1,4319 |
55,524 |
1,4100 |
45,130 |
1,4155 |
47,819 |
1,4210 |
50,454 |
1,4265 |
53,037 |
1,4320 |
55,570 |
1,4101 |
45,179 |
1,4156 |
47,868 |
1,4211 |
50,502 |
1,4266 |
53,083 |
1,4321 |
55,616 |
1,4102 |
45,228 |
1,4157 |
47,916 |
1,4212 |
50,549 |
1,4267 |
53,130 |
1,4322 |
55,661 |
1,4103 |
45,278 |
1,4158 |
47,964 |
1,4213 |
50,596 |
1,4268 |
53,176 |
1,4323 |
55,707 |
1,4104 |
45,327 |
1,4159 |
48,013 |
1,4114 |
50,644 |
1,4269 |
53,223 |
1,4324 |
55,752 |
1,4105 |
45,376 |
1,4160 |
48,061 |
1,4215 |
50,691 |
1,4270 |
53,269 |
1,4325 |
55,798 |
1,4106 |
45,426 |
1,4161 |
48,109 |
1,4216 |
50,738 |
1,4271 |
53,316 |
1,4326 |
55,844 |
1,4107 |
45,475 |
1,4162 |
48,158 |
1,4217 |
50,786 |
1,4272 |
53,362 |
1,4327 |
55,889 |
1,4108 |
45,524 |
1,4163 |
48,206 |
1,4218 |
50,833 |
1,4273 |
53,408 |
1,4328 |
55,935 |
1,4109 |
45,574 |
1,4164 |
48,254 |
1,4219 |
50,880 |
1,4274 |
53,455 |
1,4329 |
55,980 |
1,4330 |
56,026 |
1,4385 |
58,503 |
1,4440 |
60,935 |
1,4495 |
63,324 |
1,4550 |
65,672 |
1,4331 |
56,071 |
1,4386 |
58,547 |
1,4441 |
60,979 |
1,4496 |
63,367 |
1,4551 |
65,714 |
1,4332 |
56,116 |
1,4387 |
58,592 |
1,4442 |
61,023 |
1,4497 |
63,410 |
1,4552 |
65,756 |
1,4333 |
56,162 |
1,4388 |
58,637 |
1,4443 |
61,066 |
1,4498 |
63,453 |
1,4553 |
65,798 |
1,4334 |
56,207 |
1,4389 |
58,681 |
1,4444 |
61,110 |
1,4499 |
63,496 |
1,4554 |
65,841 |
1,4335 |
56,253 |
1,4390 |
58,726 |
1,4445 |
61,154 |
1,4500 |
63,539 |
1,4555 |
65,883 |
1,4336 |
56,298 |
1,4391 |
58,770 |
1,4446 |
61,198 |
1,4501 |
63,582 |
1,4556 |
65,925 |
1,4337 |
56,343 |
1,4392 |
58,815 |
1,4447 |
61,241 |
1,4502 |
63,625 |
1,4557 |
65,967 |
14338 |
56,389 |
X 1,4393 |
58,859 |
1,4448 |
61,285 |
1,4503 |
63,668 |
1,4558 |
66,010 |
1,4339 |
56,434 |
1,4394 |
58,904 |
1,4449 |
61,329 |
1,4504 |
63,711 |
1,4559 |
66,052 |
1,4340 |
56,479 |
1,4395 |
58,948 |
1,4450 |
61,372 |
1,4505 |
63,754 |
1,4560 |
66,094 |
1,4341 |
56,525 |
1,4396 |
58,993 |
1,4451 |
61,416 |
1,4506 |
63,797 |
1,4561 |
66,136 |
1,4342 |
56,570 |
1,4397 |
59,037 |
1,4452 |
61,460 |
1,4507 |
63,840 |
1,4562 |
66,178 |
1,4343 |
56,615 |
1,4398 |
59,082 |
1,4453 |
61,503 |
1,4508 |
63,882 |
1,4563 |
66,221 |
1,4344 |
56,660 |
1,4399 |
59,126 |
1,4454 |
61,547 |
1,4509 |
63,925 |
1,4564 |
66,263 |
1,4345 |
56,706 |
1,4400 |
59,170 |
1,4455 |
61,591 |
1,4510 |
63,968 |
1,4565 |
66,305 |
1,4346 |
56,751 |
1,4401 |
59,215 |
1,4456 |
61,634 |
1,4511 |
64,011 |
1,4566 |
66,347 |
1,4347 |
56,796 |
1,4402 |
59,259 |
1,4457 |
61,678 |
1,4512 |
64,054 |
1,4567 |
66,389 |
1,4348 |
56,841 |
1,4403 |
59,304 |
1,4458 |
61,721 |
1,4513 |
64,097 |
1,4568 |
66,431 |
1,4349 |
56,887 |
1,4404 |
59,348 |
1,4459 |
61,765 |
1,4514 |
64,139 |
1,4569 |
66,473 |
1,4350 |
56,932 |
1,4405 |
59,392 |
1,4460 |
61,809 |
1,4515 |
64,182 |
1,4570 |
66,515 |
1,4351 |
56,977 |
1,4406 |
59,437 |
1,4461 |
61,852 |
1,4516 |
64,225 |
1,4571 |
66,557 |
1,4352 |
57,022 |
1,4407 |
59,481 |
1,4462 |
61,896 |
1,4517 |
64,268 |
1,4572 |
66,599 |
1,4353 |
57,067 |
1,4408 |
59,525 |
1,4463 |
61,939 |
1,4518 |
64,311 |
1,4573 |
66,641 |
1,4354 |
57,112 |
1,4409 |
59,569 |
1,4464 |
61,983 |
1,4519 |
64,353 |
1,4574 |
66,683 |
1,4355 |
57,157 |
1,4410 |
59,614 |
1,4465 |
62,026 |
1,4520 |
64,396 |
1,4575 |
66,725 |
1,4356 |
57,202 |
1,4411 |
59,658 |
1,4466 |
62,070 |
1,4521 |
64,439 |
1,4576 |
66,767 |
1,4357 |
57,247 |
1,4412 |
59,702 |
1,4467 |
62,113 |
1,4522 |
64,481 |
1,4577 |
66,809 |
1,4358 |
57,292 |
1,4413 |
59,746 |
1,4468 |
62,156 |
1,4523 |
64,524 |
1,4578 |
66,851 |
1,4359 |
57,337 |
1,4414 |
59,791 |
1,4469 |
62,200 |
1,4524 |
64,567 |
1,4579 |
66,893 |
1,4360 |
57,382 |
1,4415 |
59,835 |
1,4470 |
62,243 |
1,4525 |
64,609 |
1,4580 |
66,935 |
1,4361 |
57,427 |
1,4416 |
59,879 |
1,4471 |
62,287 |
1,4526 |
64,652 |
1,4581 |
66,977 |
1,4362 |
57,472 |
1,4417 |
59,923 |
1,4472 |
62,330 |
1,45X7 |
64,695 |
1,4582 |
67,019 |
1,4363 |
57,517 |
1,4418 |
59,967 |
1,4473 |
62,373 |
1,4528 |
64,737 |
1,4583 |
67,061 |
1,4364 |
57,562 |
1,4419 |
60,011 |
1,4474 |
62,417 |
1,4529 |
64,780 |
1,4584 |
67,103 |
1,4365 |
57,607 |
1,4420 |
60,056 |
1,4475 |
62,460 |
1,4530 |
64,823 |
1,4585 |
67,145 |
1,4366 |
57,652 |
1,4421 |
60,100 |
1,4476 |
62,503 |
1,4531 |
64,865 |
1,4586 |
67,186 |
1,4367 |
57,697 |
1,4422 |
60,144 |
1,4477 |
62,547 |
1,4532 |
64,908 |
1,4587 |
67,228 |
1,4368 |
57,742 |
1,4423 |
60,188 |
1,4478 |
62,590 |
1,4533 |
64,950 |
1,4588 |
67,270 |
1,4369 |
57,787 |
1,4424 |
60,232 |
1,4479 |
62,633 |
1,4534 |
64,993 |
1,4589 |
67,312 |
1,4370 |
57,832 |
1,4425 |
60,276 |
1,4480 |
62,677 |
1,4535 |
65,035 |
1,4590 |
67,354 |
1,4371 |
57,877 |
1,4426 |
60,320 |
1,4481 |
62,720 |
1,4536 |
65,078 |
1,4591 |
67,396 |
1,4372 |
57,921 |
1,4427 |
60,364 |
1,4482 |
62,763 |
1,4537 |
65,120 |
1,4592 |
67,437 |
1,4373 |
57,966 |
1,4428 |
60,408 |
1,4483 |
62,806 |
1,4538 |
65,163 |
1,4593 |
67,479 |
1,4374 |
58,011 |
1,4429, |
60,452 |
1,4484 |
62,849 |
1,4539 |
65,205 |
1,4594 |
67,521 |
1,4375 |
58,056 |
1,4430 |
60,496 |
1,4485 |
62,893 |
1,4540 |
65,248 |
1,4595 |
67,563 |
1,4376 |
58,101 |
1,4431 |
60,540 |
1,4486 |
62,936 |
1,4541 |
65,290 |
1,4596 |
67,604 |
1,4377 |
58,145 |
1,4432 |
60,584 |
1,4487 |
62,979 |
1,4542 |
65,333 |
1,4597 |
67,640 |
1,4378 |
58,190 |
1,4433 |
60,628 |
1,4488 |
63,022 |
1,4543 |
65,375 |
1,4598 |
67,688 |
1,4379 |
58,235 |
1,4434 |
60,672 |
1,4489 |
63,065 |
1,4544 |
65,417 |
1,4599 |
67,729 |
1,4380 |
58,279 |
1,4435 |
60,716 |
1,4490 |
63,108 |
1,4545 |
65,460 |
1,4600 |
67,771 |
1,4381 |
58,324 |
1,4436 |
60,759 |
1,4491 |
63,152 |
1,4546 |
65,502 |
1,4601 |
67,813 |
1,4382 |
58,369 |
1,4437 |
60,803 |
1,4492 |
63,195 |
1,4547 |
65,544 |
1,4602 |
67,854 |
1,4383 |
58,413 |
1,4438 |
60,847 |
1,4493 |
63,238 |
1,4548 |
65,587 |
1,4603 |
67,896 |
1,4384 |
58,458 |
1,4439 |
60,891 |
1,4494 |
63,281 |
1,4549 |
65,629 |
1,4604 |
67,938 |
1,4605 |
67,979 |
1,4660 |
70,249 |
1,4715 |
72,482 |
1,4770 |
74,678 |
1,4825 |
76,841 |
1,4606 |
68,021 |
1,4661 |
70,290 |
1,4716 |
72,522 |
1,4771 |
74,718 |
1,4826 |
76,880 |
1,4607 |
68,063 |
1,4662 |
70,331 |
1,4717 |
72,562 |
1,4772 |
74,758 |
1,4827 |
76,919 |
1,4608 |
68,104 |
1,4663 |
70,372 |
1,4718 |
72,602 |
1,4773 |
74,797 |
1,4828 |
76,958 |
1,4609 |
68,146 |
1,4664 |
70,413 |
1,4719 |
72,643 |
1,4774 |
74,837 |
1,4829 |
76,997 |
1,4610 |
68,187 |
1,4665 |
70,453 |
1,4720 |
72,683 |
1,4775 |
74,876 |
1,4830 |
77,036 |
1,4611 |
68,229 |
1,4666 |
70,494 |
1,4721 |
72,723 |
1,4776 |
74,916 |
1,4831 |
77,075 |
1,4612 |
68,270, |
1,4667 |
70,535 |
1,4722 |
72,763 |
1,4777 |
74,956 |
1,4832 |
77,113 |
1,4613 |
68,312 |
1,4668 |
70,576 |
1,4723 |
72,031 |
1,4778 |
74,995 |
1,4833 |
77,152 |
1,4614 |
68,353 |
1,4669 |
70,617 |
1,4724 |
72,843 |
1,4779 |
75,035 |
1,4834 |
77,191 |
1,4615 |
68,395 |
1,4670 |
70,658 |
1,4725 |
72,884 |
1,4780 |
75,074 |
1,4835 |
77,230 |
1,4616 |
68,436 |
1,4671 |
70,698 |
1,4726 |
72,924 |
1,4781 |
75,114 |
1,4836 |
77,269 |
1,4617 |
68,478 |
1,4672 |
70,739 |
1,4727 |
72,964 |
1,4782 |
75,153 |
1,1837 |
77,308 |
1,4618 |
68,519 |
1,4673 |
70,780 |
1,4728 |
73,004 |
1,4783 |
75,193 |
1,4838 |
77,347 |
1,4619 |
68,561 |
1,4674 |
70,821 |
1,4729 |
73,044 |
1,4784 |
75,232 |
1,4839 |
77,386 |
1,4620 |
68,602 |
1,4675 |
70,861 |
1,4730 |
73,084 |
1,4785 |
75,272 |
1,4840 |
77,425 |
1,4621 |
68,643 |
1,4676 |
70,902 |
1,4731 |
73,124 |
1,4786 |
75,311 |
1,4841 |
77,463 |
14622 |
68,685 |
1,4677 |
70,943 |
1,4732 |
73,164 |
1,4787 |
75,350 |
1,4842 |
77,502 |
1,4623 |
68,726 |
1,4678 |
70,984 |
1,4733 |
73,204 |
1,4788 |
75,390 |
1,4843 |
77,541 |
1,4624 |
68,768 |
1,4679 |
71,024 |
1,4734 |
73,244 |
1,4789 |
75,429 |
1,3844 |
77,580 |
1,4625 |
68,809 |
1,4680 |
71,065 |
1,4735 |
73,285 |
1,4790 |
75,469 |
1,4845 |
77,619 |
1,4626 |
68,850 |
1,4681 |
71,106 |
1,4736 |
73,325 |
1,4791 |
75,508 |
1,4846 |
77,657 |
1,4627 |
68,892 |
1,4682 |
71,146 |
1,4737 |
73,365 |
1,4792 |
75,547 |
1,4847 |
77,696 |
1,4628 |
68,933 |
1,4683 |
71,187 |
1,4738 |
73,405 |
1,4793 |
75,587 |
1,4848 |
77,735 |
1,4629 |
68,974 |
1,4684 |
71,228 |
1,4739 |
73,445 |
1,4794 |
75,626 |
1,4849 |
77,774 |
1,4630 |
69,016 |
1,4685 |
71,268 |
1,4740 |
73,485 |
1,4795 |
75,666 |
1,4850 |
77,812 |
1,4631 |
69,057 |
1,4686 |
71,309 |
1,4741 |
73,524 |
1,4796 |
75,705 |
1,4851 |
77,851 |
1,4631 |
69,098 |
1,4687 |
71,349 |
1,4742 |
73,564 |
1,4797 |
75,744 |
1,4852 |
77,890 |
1,4633 |
69,139 |
1,4688 |
71,390 |
1,4743 |
73,604 |
1,4798 |
75,784 |
1,4853 |
77,928 |
1,4634 |
69,181 |
1,4689 |
71,431 |
1,4744 |
73,644 |
1,4799 |
75,823 |
1,4854 |
77,967 |
1,4635 |
69,222 |
1,4690 |
71,471 |
1,4745 |
73,684 |
1,4800 |
75,862 |
1,4855 |
78,006 |
1,4636 |
69,263 |
1,4691 |
71,512 |
1,4746 |
73,724 |
1,4801 |
75,901 |
1,4856 |
78,045 |
1,4637 |
69,304 |
1,4692 |
71,552 |
1,4747 |
73,764 |
1,4802 |
75,941 |
1,4857 |
78,083 |
1,4638 |
69,346 |
1,4693 |
71,593 |
1,1748 |
73,804 |
1,4803 |
75,980 |
1,4858 |
78,122 |
1,4639 |
69,387 |
1,4694 |
71,633 |
1,4749 |
73,844 |
1,4804 |
76,019 |
1,4859 |
78,160 |
1,4640 |
69,428 |
1,4695 |
71,674 |
1,4750 |
73,884 |
1,4805 |
76,058 |
1,4860 |
78,199 |
1,4641 |
69,469 |
1,4696 |
71,714 |
1,4751 |
73,924 |
1,4806 |
76,098 |
1,4861 |
78,238 |
1,4642 |
69,510 |
1,4697 |
71,755 |
1,4752 |
73,963 |
1,4807 |
76,137 |
1,4862 |
78,276 |
1,4643 |
69,551 |
1,4698 |
71,795 |
1,4753 |
74,003 |
1,4808 |
76,176 |
1,4863 |
78,315 |
1,4644 |
69,593 |
1,4699 |
71,836 |
1,4754 |
74,043 |
1,4809 |
76,215 |
1,4864 |
78,353 |
1,4645 |
69,634 |
1,4700 |
71,876 |
1,4755 |
74,083 |
1,4810 |
76,254 |
1,4865 |
78,392 |
1,4646 |
69,675 |
1,4701 |
71,917 |
1,4756 |
74,123 |
1,4811 |
76,294 |
1,4866 |
78,431 |
1,4647 |
69,716 |
1,4702 |
71,957 |
1,4757 |
74,162 |
1,4812 |
76,333 |
1,4867 |
78,469 |
1,4648 |
69,757 |
1,4703 |
71,998 |
1,4758 |
74,202 |
1,4813 |
76,372 |
1,4868 |
78,508 |
1,4649 |
69,798 |
1,4704 |
72,038 |
1,4759 |
74,242 |
1,4814 |
76,411 |
1,4869 |
78,546 |
1,4650 |
69,839 |
1,4705 |
72,078 |
1,4760 |
74,282 |
1,4815 |
76,450 |
1,4870 |
78,585 |
1,4651 |
69,880 |
1,4706 |
72,119 |
1,4761 |
74,321 |
1,4816 |
76,489 |
1,4871 |
78,623 |
1,4652 |
69,921 |
1,4707 |
72,159 |
1,4762 |
74,361 |
1,4817 |
76,528 |
1,4872 |
78,662 |
1,4653 |
69,962 |
1,4708 |
72,199 |
1,4763 |
74,401 |
1,4818 |
76,567 |
1,4873 |
78,700 |
1,4654 |
70,003 |
1,4709 |
72,240 |
1,4764 |
74,441 |
1,4819 |
76,607 |
1,4874 |
78,739 |
1,4655 |
70,044 |
1,4710 |
72,280 |
1,4765 |
74,480 |
1,4820 |
76,646 |
1,4875 |
78,777 |
1,4656 |
70,085 |
1,4711 |
72,320 |
1,4766 |
74,520 |
1,4821 |
76,685 |
1,4876 |
78,816 |
1,4657 |
70,126 |
1,4712 |
72,361 |
1,4767 |
74,560 |
1,4822 |
70,724 |
1,4877 |
78,854 |
1,4658 |
70,167 |
1,4713 |
72,401 |
1,4768 |
74,599 |
1,4823 |
70,763 |
1,4878 |
78,892 |
1,4659 |
70,208 |
1,4714 |
72,441 |
1,4769 |
74,639 |
1,4824 |
76,802 |
1,4879 |
78,931 |
1,4880 |
78,969 |
1,4920 |
80,497 |
1,4960 |
82,007 |
1,5000 |
83,500 |
1,5040 |
84,976 |
1,4881 |
79,008 |
1,4921 |
80,534 |
1,4961 |
82,044 |
1,5001 |
83,537 |
1,5041 |
85,013 |
1,4882 |
79,046 |
1,4922 |
80,572 |
1,4962 |
82,082 |
1,5002 |
83,574 |
1,5042 |
85,049 |
1,4883 |
79,084 |
1,4923 |
80,610 |
1,4963 |
82,119 |
1,5003 |
83,611 |
1,5043 |
85,086 |
1,4884 |
79,123 |
1,4924 |
80,648 |
1,4964 |
82,157 |
1,5004 |
83,648 |
1,5044 |
85,123 |
1,4885 |
79,161 |
1,4925 |
80,686 |
1,4965 |
82,194 |
1,5005 |
83,685 |
1,5045 |
85,159 |
1,4886 |
79,199 |
1,4926 |
80,724 |
1,4966 |
82,232 |
1,5006 |
83,722 |
1,5046 |
85,196 |
1,4887 |
79,238 |
1,4927 |
80,762 |
1,4967 |
82,269 |
1,5007 |
83,759 |
1,5047 |
85,233 |
1,4888 |
79,276 |
1,4928 |
80,800 |
1,4968 |
82,307 |
1,5008 |
83,796 |
1,5048 |
85,269 |
1,4889 |
79,314 |
1,4929 |
80,838 |
1,4969 |
82,344 |
1,5009 |
83,833 |
1,5049 |
85,306 |
1,4890 |
79,353 |
1,4930 |
80,876 |
1,4970 |
82,381 |
1,5010 |
83,870 |
1,5050 |
85,343 |
1,4891 |
79,391 |
1,4931 |
80,913 |
1,4971 |
82,419 |
1,5011 |
83,907 |
1,5051 |
85,379 |
1,4892 |
79,429 |
1,4932 |
80,951 |
1,4972 |
82,456 |
1,5012 |
83,944 |
1,5052 |
85,416 |
1,4893 |
79,468 |
1,4933 |
80,989 |
1,4973 |
82,494 |
1,5013 |
83,981 |
1,5053 |
85,452 |
1,4894 |
79,506 |
1,4934 |
81,027 |
1,4974 |
82,531 |
1,5014 |
84,018 |
1,5054 |
85,489 |
1,4895 |
79,544 |
1,4935 |
81,065 |
1,4975 |
82,569 |
1,5015 |
84,055 |
1,5055 |
85,525 |
1,4596 |
79,582 |
1,4936 |
81,103 |
1,4976 |
82,606 |
1,5016 |
84,092 |
1,5056 |
85,562 |
1,4597 |
79,620 |
1,4937 |
81,140 |
1,4977 |
82,643 |
1,5017 |
84,129 |
1,5057 |
85,598 |
1,4898 |
79,659 |
1,4938 |
81,178 |
1,4978 |
32,681 |
1,5018 |
84,166 |
1,5058 |
85,635 |
1,4899 |
79,697 |
1,4939 |
81,216 |
1,4979 |
82,718 |
1,5019 |
84,203 |
1,5059 |
85,672 |
1,4900 |
79,735 |
1,4940 |
81,254 |
1,4980 |
82,755 |
1,5020 |
84,240 |
1,5060 |
85,708 |
1,4901 |
79,773 |
1,4941 |
81,291 |
1,4981 |
82,793 |
1,5021 |
84,277 |
1,5061 |
85,744 |
1,4902 |
79,811 |
1,4942 |
81329 |
1,4982 |
82,830 |
1,5022 |
84,314 |
1,5062 |
85,781 |
1,4903 |
79,850 |
1,4943 |
81,367 |
1,4983 |
82,867 |
1,5023 |
84,351 |
1,5063 |
85,817 |
1,4904 |
79,888 |
1,4944 |
81,405 |
1,4984 |
82,905 |
1,5024 |
84,388 |
1,5064 |
85,854 |
1,4905 |
79,926 |
1,4945 |
81,442 |
1,4985 |
82,942 |
1,5025 |
84,424 |
1,5065 |
85,890 |
1,4906 |
79,964 |
1,4946 |
81,480 |
1,4986 |
82,979 |
1,5026 |
84,461 |
1,5066 |
85,927 |
1,4907 |
80,002 |
1,4947 |
81,518 |
1,4987 |
83,016 |
1,5027 |
84,498 |
1,5067 |
85,963 |
1,4908 |
80,040 |
1,4948 |
81,555 |
1,4988 |
83,054 |
1,5028 |
84,535 |
1,5068 |
86,000 |
1,4909 |
80,078 |
1,4949 |
81,593 |
1,4989 |
83,091 |
1,5029 |
84,572 |
1,5069 |
86,036 |
1,4910 |
80,116 |
1,4950 |
81,631 |
1,4990 |
83,128 |
1,5030 |
84,609 |
1,5070 |
86,072 |
1,4911 |
80,154 |
1,4951 |
81,668 |
1,4991 |
83,165 |
1,5031 |
84,645 |
1,5071 |
86,109 |
1,4912 |
80,192 |
1,4952 |
81,706 |
1,4992 |
83,202 |
1,5032 |
84,682 |
1,5072 |
86,145 |
1,4913 |
80,231 |
1,4953 |
81,744 |
1,4993 |
83,240 |
1,5033 |
84,719 |
1,5073 |
86,182 |
1,4914 |
80,269 |
1,4954 |
81,781 |
1,4994 |
83,277 |
1,5034 |
84,756 |
1,5074 |
86,218 |
1,4915 |
80,307 |
1,4955 |
81,819 |
1,4995 |
83,314 |
1,5035 |
84,792 |
1,5075 |
86,254 |
1,4916 |
80,345 |
1,4956 |
81,856 |
1,4996 |
83,351 |
1,5036 |
84,829 |
1,5076 |
86,291 |
1,4917 |
80,383 |
1,4957 |
81,894 |
1,4997 |
83,388 |
1,5037 |
84,866 |
1,5077 |
86,327 |
1,4918 |
80,421 |
1,4958 |
81,932 |
1,4998 |
83,425 |
1,5038 |
84,903 |
1,5078 |
86,363 |
1,4919 |
80,459 1 |
1,4959 |
81,969 |
1,4999 |
83,463 1 |
1,5039 |
84,939 |
1,5079 |
86,399 |
Xxxxx xxxxxxxxx x šarži xxxx xxxxx xxxxx |
Xxxxx xxxxxxxxx, které musí xxx odebrány |
1 xx 25 |
Xxxxxxx 1 xxxxxxxxx |
26 xx 100 |
xxxxxxx 2 xxxxxxxxx |
&xx; 100 |
5 xxxxxxxxx |
Xxxxxxxx šarže (xx) |
Xxxxxxxxx xxxxx xxxxxxx vzorků, xxxxx má xxx xxxxxxx |
&xx; 50 |
3 |
50 xx 500 |
5 |
&xx; 500 |
10 |
Xxxxx balení xxxx xxxxxxxx x šarži |
Počet xxxxxx xxxx xxxxxxxx, xxxxx má xxx xxxxxxx |
1 až 25 |
1 xxxxxx xxxx xxxxxxxx |
26 xx 100 |
xxx 5 %, xxxxxxx 2 xxxxxx xxxx jednotky |
> 100 |
xxx 5 %, xxxxxxxxx 10 xxxxxx xxxx xxxxxxxx |
Xxxxxxxx |
Xxxxxxx a xxxxxxxx |
Xxxxxxxxxxxx |
Xxxxxxxxx specifikované v xxxxxxxx (XX) x. 242/2004 |
Xxx xxxxxxxxxxxxxxxx |
Xxxxx xxxx xxxxx 5 xx/xx |
Xxx xxxxxxxxxxxxxxx |
Xxxxx xxxx xxxxx 10 xx/xx |
Xxxxxxxx |
Xxxxxxx XXXXXXx xxxx HORRATR dosažené xx validační kolaborativní xxxxxx xxxx xxx xxxxx xxx 1,5 |
Xxxxxxxxx |
80 % až 105 % (dosažená v xxxxxxxxxxxxx xxxxxx) |
Xxxxxxxxxxxx |
Xxxxxxxxx nesmí xxx xxxxxx matricovými x spektrálními xxxx |
Množství µx/xx |
Xxxxxxx |
||
XXXx % |
XXXX % |
Xxxxxxxxx % |
|
< 20 |
≤ 30 |
≤ 40 |
50 xx 120 |
20-50 |
≤ 20 |
≤ 30 |
70 až 105 |
> 50 |
≤ 15 |
≤ 25 |
75 xx 105 |
Xxxxxxxx xxxxx (xx)
|
Xxxxxxxxx xxxxx dílčích xxxxxx, xxxxx xxxx být xxxxxxxx
|
&xx; 50
|
3
|
50 xx 500
|
5
|
&xx; 500
|
10
|
Xxxxx xxxxxx nebo xxxxxxxx x xxxxx
|
Xxxxx xxxxxx xxxx jednotek, xxxxx xxxx být xxxxxxxx
|
1 xx 25
|
1 xxxxxx nebo jednotka
|
26 xx 100
|
xxx 5 %, xxxxxxx 2 xxxxxx xxxx xxxxxxxx
|
&xx; 100
|
xxx 5 %, xxxxxxxxx 10 balení xxxx xxxxxxxx
|
Xxxxxxxx
|
Xxxxxxx/xxxxxxxx
|
Xxxxxxxxxxxx
|
Xxxxxxxxx xxxxxxxxxxxxx v nařízení (XX) č. 208/2005
|
Xxx xxxxxxxxxxxxxxxx
|
Xxxxx xxxx xxxxx 0,3 μx/xx
|
Xxx stanovitelnosti
|
Nižší xxxx xxxxx 0,9 μg/kg
|
Přesnost
|
Hodnoty XXXXXXx nebo XXXXXXX xxxxxxxx xx xxxxxxxxx xxxxxxxxxxxxx xxxxxx musí xxx xxxxx xxx 1,5
|
Xxxxxxxxx
|
50 % xx 120 %
|
Xxxxxxxxxxxx
|
Xxxxxxxxx xxxxx xxx xxxxxx xxxxxxxxxxx x xxxxxxxxxxxx jevy, xxxxxxx xxxxxxx
|
Xxxxxxxx
|
Xxxxxxxxxx xxxxx (x)
|
Xxxxxxxx nebo xxxxx xxxxx xxxxx
|
Xxxxx xxxxxxx xxxxxx
|
Xxxxxxxx xxxxxxxxxx xxxxxx (xx)
|
Xxxxxxxxx x xxxxxxx x obilovin
|
≥ 1500
|
500 x
|
100
|
10
|
&xx; 300 x &xx; 1500
|
3 xxxxx xxxxx
|
100
|
10
|
|
≥ 50 a ≤ 300
|
100 t
|
100
|
10
|
|
< 50
|
-
|
3 - 100*)
|
1 - 10
|
|
*) v závislosti xx xxxxxxxxx šarže - xxx xxxxxxx 2
|
Xxxxxxxx xxxxx (x)
|
Xxxxx xxxxxxx xxxxxx
|
≤ 0,05
|
3
|
&xx; 0,05 - ≤ 0,50
|
5
|
&xx; 0,50 - ≤ 1,00
|
10
|
&xx; 1,00 - ≤ 3,00
|
20
|
&xx; 3,00 - ≤ 10,00
|
40
|
&xx; 10,00 - ≤ 20,00
|
60
|
&xx; 20,00 - ≤ 50,00
|
100
|
Xxxxxxxx μg/kg
|
deoxynivalenol
|
||
|
RSDr %
|
XXXX %
|
Xxxxxxxxx %
|
> 100,00 - ≤ 500,00
|
≤ 20,00
|
≤ 40,00
|
60,00 - 110,00
|
&xx; 500,00
|
≤ 20,00
|
≤ 40,00
|
70,00 - 120,00
|
Xxxxxxxx μx/xx
|
xxxxxxxxxx
|
||
&xxxx;
|
XXXx %
|
XXXX %
|
Výtěžnost %
|
≤ 50,00
|
≤ 40,00
|
≤ 50,00
|
60,00 - 120,00
|
> 50,00
|
≤ 25,00
|
≤ 40,00
|
70,00 - 120,00
|
Xxxxxxxx μx/xx
|
Xxxxxxx X1 xxxx X2
|
||
&xxxx;
|
XXXx %
|
RSDR %
|
Xxxxxxxxx %
|
≤ 500,00
|
≤ 30,00
|
≤ 60,00
|
60,00 - 120,00
|
&xx; 550,00
|
≤ 20,00
|
≤ 30,00
|
70,00 - 110,00
|
Xxxxxxxx μx/xx
|
X-2 toxin
|
||
|
RSDr %
|
XXXX %
|
Xxxxxxxxx %
|
50,00 - 250,00
|
≤ 40,00
|
≤ 60,00
|
60,00 - 130,00
|
> 250,00
|
≤ 30,00
|
≤ 50,00
|
70,00 - 130,00
|
&xxxx;
|
&xxxx;
|
&xxxx;
|
&xxxx;
|
Xxxxxxxx μx/xx
|
XX-2 toxin
|
||
|
RSDr %
|
XXXX %
|
Výtěžnost %
|
100,00 - 200,00
|
≤ 40,00
|
≤ 60,00
|
60,00 - 130,00
|
> 200,00
|
≤ 30,00
|
≤ 50,00
|
70,00 - 130,00
|
C (μx/xx)
|
α
|
≤ 50,00
|
0,20
|
51,00 - 500,00
|
0,18
|
501,00 - 1000,00
|
0,15
|
1001,00 - 10000,00
|
0,12
|
&xx; 10000,00
|
0,10
|